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    Mechanical Milling a Top Down Approach for the Synthesis . First the amorphous boron powder was ball milling for 150 h at room temperature in ammonia gas and then annealed in NH 3 gas at 1200℃ for 8 h Figure 12a is the SEM images of as obtained milled powder and Figure 12b reveals a large number of thin fibers from the surface of the aggregates clusters

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